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Reaction of nitric oxide with benzyl cyanide to yield a bis- diazeniumdiolated imidate

  1. Author:
    Arnold, E. V.
    Keefer, L. K.
    Hrabie, J. A.

  2. Author Address

    NCI, Frederick Canc Res & Dev Ctr, Comparat Carcinogenesis Lab, Chem Sect, Frederick, MD 21702 USA. NCI, Frederick Canc Res & Dev Ctr, Comparat Carcinogenesis Lab, Chem Sect, Frederick, MD 21702 USA. NCI, Frederick Canc Res & Dev Ctr, SAIC Frederick, Frederick, MD 21702 USA.
    1. Year: 2000
  2. Journal: Tetrahedron Letters
    1. 41
    2. 44
    3. Pages: 8421-8424
  4. Type of Article: Article
  1. Abstract:

    The reaction of nitric oxide with benzyl cyanide in the presence of sodium methoxide forms the bis-diazeniumdiolated imidate, PhC[C(OMe)=NH][N(O)NO-Na+](2). This compound decomposes in acidic media to yield nitric oxide, nitrous oxide and 2-oximino-2-phenylacetic acid methyl ester. (C) 2000 Elsevier Science Ltd. All rights reserved.

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