Skip NavigationSkip to Content
Return Return to Search Results

Analysis of stibonic acids by ion exchange chromatography with ESI-MS/photodiode array detection

  1. Author:
    Simmons, T. L.
    McCloud, T. G.

  2. Author Address

    NCI, SAIC Frederick Inc, Frederick Canc Res & Dev Ctr, Frederick, MD 21702 USA NCI, SAIC Frederick Inc, Frederick Canc Res & Dev Ctr, Frederick, MD 21702 USA McCloud TG NCI, SAIC Frederick Inc, Frederick Canc Res & Dev Ctr, Frederick, MD 21702 USA
    1. Year: 2003
  2. Journal: Journal of Liquid Chromatography & Related Technologies
    1. 26
    2. 13
    3. Pages: 2041-2051
  4. Type of Article: Article
  1. Abstract:

    A method utilizing the counter anion exchange properties of aqueous ammonium acetate at pH 9, increasing in concentration linearly from 0 to 0.1 M NH4OAc, using a Hamilton PRP-X100 anion exchange column, is presented for the resolution of aromatic stibonic acids and their detection by UV and ESI mass spectrometry. Additional phase-bonded silica or polymer backed C-8 and C-18 column types, eluted with various counter ion solutions (KClO4, NH4COOH, NaOH, NaH2PO4) were evaluated for suitability for stibonic acid analysis.

    See More

  1. Keywords:

External Sources

  1. No sources found.

Library Notes

  1. No notes added.
NCI at Frederick

You are leaving a government website.

This external link provides additional information that is consistent with the intended purpose of this site. The government cannot attest to the accuracy of a non-federal site.

Linking to a non-federal site does not constitute an endorsement by this institution or any of its employees of the sponsors or the information and products presented on the site. You will be subject to the destination site's privacy policy when you follow the link.

ContinueCancel